TITLE Celtis africana metabolite profiles: Supplementary Materials PRESENTATION OF DATA Tables DATA FORMAT Raw and filtered INSTRUMENT FEATURES AND MODEL Pegasus 4D two-dimensional gas chromatography coupled with time of flight mass spectrometry (GCxGC-TOF-MS) (LECO Corporation, Michigan, USA) fitted with a Rxi-5Sil MS (30 m, 250 µm i.d., 0.25 µm df) (Restek, Pennsylvania, USA) primary column and a Rxi-17Sil MS (2 m, 250 µm i.d., 0.25 µm df) (Restek, Pennsylvania, USA) secondary column. METHOD Fungal and bacterial endophytes were isolated from aerial parts of Celtis africana. Crude extracts from endophytes were prepared by extracting fermented broth cultures with ethyl acetate, hexane and dichloromethane. Plant crude extracts from the stems, leaves and fruits were prepared by extracting with ethyl acetate, hexane and dichloromethane : methanol (1:1, v/v). Untargeted metabolite profiling was performed using GCxGC-TOF-MS. Spectral data was analyzed using ChromaTOF software (LECO Corporation, Michigan, USA) and was filtered in Microsoft Excel (Microsoft Corporation, USA). RELATED RESEARCH ARTICLE K.I. Tapfuma, E.K. Nchabaleng, O.A. Adebo, R. Hussan, R.D. Williams, A.B. Ravuluvulu, D.T. Ndinteh, R.Y. Gan, O. Habimana, N. Niemann, F.M. Muganza, L. Mekuto, V. Mavumengwana. Antibacterial activity and gas chromatography mass spectrometry (GC-MS)-based metabolite profiles of Celtis africana and its endophytic extracts. Industrial Crops and Products [In Press].